Abstract

Aging performance of polyethylene (PE) material from PE pipe under hydrostatic pressure was investigated by measuring its mechanical/chemical properties. Tensile test, thermogravimetric analysis (TGA), oxidation induction time (OIT), as well as hardness test were carried out to evaluate the aging status of polyethylene material. Results show that as aging time prolongs, elongation rate after brake, thermal decomposition temperature, as well as oxidation induction time of PE specimen decrease, while its hardness increases, indicating that its mechanical/chemical properties change with the aging intensity. Life prediction model was also established based on failure time–pressure data obtained from hydrostatic pressure test, under the guidance of Arrhenius theory. Conclusions drawn from this research could help to prompt the efficiency of PE pipe on-site inspection as well as serve as references for understanding the aging behavior of PE pipe.

References

1.
Yun
,
L. U.
,
Lei
,
Z.
, and
Hui-Min
,
T.
,
2006
, “
Effect of Light Stabilizer Containing Stable Nitroxyl Oxides of Free Radical on Light Aging-Resistance of PE/EVA Films
,”
China Plastic
, 20(4), pp.
95
99
.
2.
Peng-Cheng
,
F.
,
Jian-Ying
,
Y. U.
,
Xi-Lin
,
W.
, and
Gui-Ping
,
Z.
,
2009
, “
Aging Properties of PE/CPE/PVC Ternary Blends
,”
J. Wuhan Univ. Technol.
,
31
(
23
), pp.
23
26
.10.3963/j.issn.1671-4431.2009.23.006
3.
Kratochvilla
,
T. R.
,
Frank
,
A.
, and
Pinter
,
G.
,
2014
, “
Determination of Slow Crack Growth Behaviour of Polyethylene Pressure Pipes With Cracked Round Bar Test
,”
Polym. Test.
,
40
, pp.
299
303
.10.1016/j.polymertesting.2014.10.002
4.
Wang
,
Y.
,
Lan
,
H.
, and
Meng
,
T.
,
2019
, “
Lifetime Prediction of Natural Gas Polyethylene Pipes With Internal Pressures
,”
Eng. Failure Anal.
,
95
, pp.
154
163
.10.1016/j.engfailanal.2018.09.022
5.
Wang
,
Y.
,
Lan
,
H. Q.
, and
Zhang
,
H.
,
2019
, “
A Residual Lifetime Prediction Method of Aging Polyethylene Gas Pipes in Service
,”
ASME
Paper No. PVP2019-93140.10.1115/PVP2019-93140
6.
Zha
,
S.
,
Lan
,
H. Q.
,
Lin
,
N.
, and
Meng
,
T.
,
2023
, “
Degradation and Characterization Methods for Polyethylene Gas Pipes After Natural and Accelerated Aging
,”
Polym. Degrad. Stab.
,
208
, p.
110247
.10.1016/j.polymdegradstab.2022.110247
7.
Jun
,
W.
, and
Jian
,
P.
,
2005
,
Study on Structure and Mechanical Properties of PE-HD During the Aging Test
,
China Plastics
, 12(1), pp.
46
49
.
8.
Cao
,
F. Q.
,
Li
,
X. H.
,
Liu
,
Z. C.
,
Li
,
Y. L.
, and
Yun
,
S.
,
2015
, “
Low Temperature Accelerated Aging Study of Propellant Charge in Structural Tester
,”
Chin. J. Energetic Mater.
, 23(7), pp.
648
652
.10.11943/j.issn.1006-9941.2015.07.008
9.
Wang
,
Q.
,
Zhou
,
H.
,
Xie
,
J.
, and
Xu
,
X.
,
2021
, “
Nonlinear Ultrasonic Evaluation of High-Density Polyethylene Natural Gas Pipe Thermal Butt Fusion Joint Aging Behavior
,”
Int. J. Pressure Vessels Piping
,
189
(
1
), p.
104272
.10.1016/j.ijpvp.2020.104272
10.
Redhead
,
A.
,
Frank
,
A.
, and
Pinter
,
G.
,
2011
, “
Investigation of the Chemical Resistance and the Material Aging Conditions of Polyethylene for Pipe Applications
,”
EUROTEC 2011 Conference, in Conjunction With EQUIPLAST
, Barcelona, Spain, Nov. 14–15, p.
5
.https://pure.unileoben.ac.at/en/publications/investigation-of-the-chemical-resistance-and-the-material-aging-c
11.
Bredács
,
M.
,
Frank
,
A.
,
Bastero
,
A.
,
Stolarz
,
A.
, and
Pinter
,
G.
,
2018
, “
Accelerated Aging of Polyethylene Pipe Grades in Aqueous Chlorine Dioxide at Constant Concentration
,”
Polym. Degrad. Stab.
,
157
, pp.
80
89
.10.1016/j.polymdegradstab.2018.09.019
12.
Lin
,
D.
,
Cen
,
K.
,
Pu
,
C. X.
,
Hu
,
X.
, and
Shao
,
C. C.
,
2019
, “
Study on Evaluation Indicators of Aging Performance of Gas Polyethylene Pipe in Service
,”
Gas Heat
, 12(5), pp.
43
51
.
13.
Ulloa
,
A. H.
,
D'Almeida
,
J. R. M.
, and
Habas
,
J. P.
,
2010
, “
Creep Behavior of High Density Polyethylene After Aging in Contact With Different Oil Derivates
,”
Polym. Eng. Sci.
,
50
(
11
), pp.
2122
2130
.10.1002/pen.21743
14.
Dai
,
J.
,
Yan
,
H.
,
Wang
,
X.
,
Guo
,
J.
,
Hu
,
Z.
, and
Yang
,
J.
,
2017
, “
Grey Correlation Analysis of Influencing Factors of Polyethylene Thermo-Oxidation Aging Based on AHP-DEA
,”
Chem. Ind. Eng. Prog.
, 36(4), pp.
1358
1365
.https://hgjz.cip.com.cn/EN/10.16085/j.issn.1000-6613.2017.04.027
15.
Dai
,
J.
,
Yan
,
H.
,
Guo
,
J.
,
Hu
,
Z.
, and
Yang
,
J.
,
2016
, “
Analysis of Degradation Properties of Low Density Polyethylene After Thermo-Oxidative Aging Based on TGA and DSC-SSA
,”
Mater. Rev.
, 33(22), pp.
349
352, 368
.
16.
Lan
,
H.
,
Sha
,
D.
,
Meng
,
T.
,
Fang
,
X.
, and
Li
,
X.
,
2016
, “
Thermal Oxidative Aging Laws of PE Gas Pressure Pipes
,”
Nat. Gas Ind.
, 36(2), pp.
78
83
.10.3787/j.issn.1000-0976.2016.04.012
17.
Chen
,
G.
,
Yang
,
Y.
,
Zhou
,
C.
,
Zhou
,
Z.
, and
Yan
,
D.
,
2019
, “
Thermal‐Oxidative Aging Performance and Life Prediction of Polyethylene Pipe Under Cyclic and Constant Internal Pressure
,”
J. Appl. Polym. Sci.
,
136
(
28
), p.
47766
.10.1002/app.47766
18.
Xinwei
,
W.
,
Yumei
,
Z.
,
Ping
,
W.
,
Xiuhong
,
H.
, and
Jingan
,
X.
,
2013
, “
Study on Test Method of PE-UHMW Tensile Creep Properties
,”
Eng. Plast. Appl.
, 41(11), pp.
88
91
.
19.
Real
,
L. E. P.
, and
Correia
,
M. B.
,
2012
, “
A Comparative Study on the Thermo-Oxidative Stability of Polyethylene
,”
Polym. Test.
,
31
(
7
), pp.
963
969
.10.1016/j.polymertesting.2012.07.005
20.
Boros
,
S. J.
,
2009
, “
Long-Term Strength and Design of Polyethylene Compounds for Pressure Pipe Applications
,”
ASME
Paper No. ICONE17-76052.10.1115/ICONE17-76052
21.
Lee
,
H. J.
, and
Kim
,
W.
,
2020
, “
Long-Term Durability Evaluation of Fiber-Reinforced ECC Using Wood-Based Cellulose Nanocrystals
,”
Constr. Build. Mater.
,
238
, p.
117754
.10.1016/j.conbuildmat.2019.117754
22.
Mattos
,
H.
,
Reis
,
J.
,
Amorim
,
F. C.
,
Brandao
,
J.
,
Lana
,
L.
, and
Perrut
,
V. A.
,
2021
, “
Long-Term Field Performance of a Composite Pipe Repair Under Constant Hydrostatic Pressure
,”
Eng. Failure Anal.
,
130
, p.
105765
.10.1016/j.engfailanal.2021.105765
23.
Chen
,
J.
, and
Liu
,
Y.
,
2019
, “
Probabilistic Aging Pipe Strength Estimation Using Multimodality Information Fusion
,”
Prognostics Health Manage. Soc.
, 2(8), pp.
1
8
.10.36001/phmconf.2019.v11i1.817
24.
Deya
,
B. M.
,
Sattar
,
A.
,
Aslan
,
M. H.
, and
Oral
,
A. Y.
,
2011
, “
Study of the Environmental Effect on Creep Test of PE Blends
,”
AIP Conf. Proc.
, pp.
227
231
.10.1063/1.3663118
25.
Reyes-Labarta
,
J. A.
,
Olaya
,
M. M.
, and
Marcilla
,
A.
,
2006
, “
DSC and TGA Study of the Transitions Involved in the Thermal Treatment of Binary Mixtures of PE and EVA Copolymer With a Crosslinking Agent
,”
Polymer
,
47
(
24
), pp.
8194
8202
.10.1016/j.polymer.2006.09.054
26.
Majewsky
,
M.
,
Horn
,
H.
,
Bitter
,
H.
, and
Eiche
,
E.
,
2016
, “
Determination of Microplastic Polyethylene (PE) and Polypropylene (PP) in Environmental Samples Using Thermal Analysis (TGA-DSC)
,”
Sci. Total Environ.
,
568
, pp.
507
511
.10.1016/j.scitotenv.2016.06.017
You do not currently have access to this content.